(Solved): what is the TLC value for the starting materials and products?Do the FTIR amd NMR spectra you measur ...

For this assignment, the target compound that you should synthesize is 3-chloro-1-butene. A gain, this is an electropailic alkeoe addition reaction. Frumine the prodoct to deternine the location of the new functionality. Keep in mind the nature of the intermediate. The regioselectivity is controlled by the stability of this internedate Assume flat naly ose equivalent of reageat is used. Synthesis Procedures 1. To start this activity, click this link for Diene Halogenation - 1 ts. The lab will load in a new tab. Click back to this tab to read further instructions and contiplete the questians below. Use the available reagents in the Alkene Bromination section of the Stockroom tab and identify the appropriale starting materials required to syntherize the target compound and add them to the round bottom flask. Now add ether \( \left(\mathrm{Ft}_{2} \mathrm{O}\right) \) as a solvent and drag the flatk 10 the Stir Plate on the labbench. 2. The contents of the flask will be visible in Live Data. From the group of reagents foend on the lab bench, select the coirect reagent to synthesire the taget compound and add it to the flask on the stir plate. Now pat the round bottom flask in the ice bath so the reaction mixtare can be cooled. 3. Start the reaction by clicking on the dials on the front of the stir plate. You should be able to obierve the reaction mixture stirring in the rlask. Monitor the progress of the reaction asing TLC measurements as necessary until the product has formed and the starting materials have been coesarmed (if you have not previoasly completed the activity Using Thin Layer Chromatography, please see the note at the bottom of that assignment reganding TLC in Beyond Labs.). You can atvance the liboratory time uning be dock on the wall. You can also save your TI.C plates by clicking Save on the TLC window. 4. When the reaction is complete, "work up" your reaction by doing a separatory farnel extraction. Drag and drop the separnoory funinel on the flakk and then ads the appropriade solvent to the funnel. Remember that the addition of any açeous solvent also ad4s diethyl cther, although this is not aboun (sco note at the boetom of the activify Perfening a Separatory Funnel Extraction). Enther the organic or the aqueous layer can be semoved by clicking and draging it to the bench. Your target conipound ahould be is coe of there layers. The other layer can be discarded into the red bin. Wis the starting materials, solvert, reogent, and prodacts formed: Remiember that subscripes \( \left(A_{B}\right) \) and saperscripts \( \left(A^{B}\right) \) can be incladed as needed wsing the _ and A chanacters rempecticly.